New electroanalytical methods for voltammetric determination of paraquat were developed using DC voltammetry (DCV) and differential pulse voltammetry (DPV) at a meniscus modified silver solid amalgam electrode (m-AgSAE). Optimal conditions were found in Britton-Robinson (BR) buffer pH 11 without regeneration of working electrode within the concentration range 1.10-4 – 1.10-7 mol.l-1.