Phase Transformations and Recrystallization in Cold-Rolled Al-Mg-Sc-Zr Alloy Prepared by Powder Metallurgy
Abstract
The mechanical, thermal and electrical properties and recrystallization behaviour of the cold-rolled AlMgScZr alloy prepared by powder metallurgy were studied. The materials were investigated during isothermal annealing (400 and 550 °C) and during step-by-step linear annealing from room temperature up to 570 °C.
The observed results were compared with microstructure observation by transmission electron microscopy and electron diffraction from a previous study of the Al-Mg-based alloys with Sc and Zr. The precipitation sequence of the Al-Mg system and coarsening of the Sc,Zr-containing particles caused electrical and heat flow changes during the annealing.
The presence of the Al3(Sc,Zr) particles has an anti-recrystallization effect that prevents recrystallization at temperature minimally up to TILDE OPERATOR+D91 400 °C. A partial recrystallization of the alloy was registered after annealing at 550 °C already for 30 min.
The cause of the anti-recrystallization effect is precipitation of the Mg-containing particles as follows from a comparison to the alloy without Mg. But the Mg-addition to the Al-Sc-Zr alloy prepared by powder metallurgy has a poorer anti-recrystallization effect than a Mn-addition.